ASTM E509/E509M-21

3.1?Reactor vessels made of ferritic steels are designed with the expectation of progressive changes in material properties resulting from in-service neutron exposure. In the operation of light-water-cooled nuclear power reactors, changes in pressure-temperature (P T) limits are made periodically during service life to account for the effects of neutron radiation on the ductile-to-brittle transition temperature material properties. If the degree of neutron embrittlement becomes large, the restrictions on operation during normal heat-up and cool down may become severe. Additional consideration should be given to postulated events, such as pressurized thermal shock (PTS). A reduction in the upper shelf toughness also occurs from neutron exposure, and this decrease may reduce the margin of safety against ductile fracture. When it appears that these situations could develop, certain alternatives are available that reduce the problem or postpone the time at which plant restrictions must be considered. One of these alternatives is to thermally anneal the reactor vessel beltline region, that is, to heat the beltline region to a temperature sufficiently above the normal operating temperature to recover a significant portion of the original fracture toughness and other material properties that were degraded as a result of neutron embrittlement.

3.2?Preparation and planning for an in-service anneal should begin early so that pertinent information can be obtained to guide the annealing operation. Sufficient time should be allocated to evaluate the expected benefits in operating life to be gained by annealing; to evaluate the annealing method to be employed; to perform the necessary system studies and stress evaluations; to evaluate the expected annealing recovery and reembrittlement behavior; to develop and functionally test such equipment as may be required to do the in-service annealing; and, to train personnel to perform the anneal.

3.3?Selection of the annealing temperature requires a balance of opposing conditions. Higher annealing temperatures, and longer annealing times, can produce greater recovery of fracture toughness and other material properties and thereby increase the post-anneal lifetime. The annealing temperature also can have an impact on the reembrittlement trend after the anneal. On the other hand, higher temperatures can create other undesirable property effects such as permanent creep deformation or temper embrittlement. These higher temperatures also can cause engineering difficulties, that is, core and coolant removal and storage, localized heating effects, etc., in preventing the annealing operation from distorting the vessel or damaging vessel supports, primary coolant piping, adjacent concrete, insulation, etc. See ASME Code Case N-557 for further guidance on annealing conditions and thermal-stress evaluations (2).

3.4?Throughout the annealing operation, accurate measurement of the annealing temperature at key defined locations must be made and recorded for later engineering evaluation.

3.5?After the annealing operation has been carried out, several steps should be taken. The predicted improvement in fracture toughness properties must be verified, and it must be demonstrated that there is no damage to key components and structures.

3.6?Further action may be required to demonstrate that reactor vessel integrity is maintained within ASME Code requirements such as indicated in the referenced ASME Code Case N-557 1.1?This guide covers the general procedures for conducting an in-service thermal anneal of a light-water moderated nuclear reactor vessel and demonstrating the effectiveness of the procedure. The purpose of this in-service annealing (heat treatment) is to improve the mechanical properties, especially fracture toughness, of the reactor vessel materials previously degraded by neutron embrittlement. The improvement in mechanical properties generally is assessed using Charpy V-notch impact test results, or alternatively, fracture toughness test results or inferred toughness property changes from tensile, hardness, indentation, or other miniature specimen testing 1.2?This guide is designed to accommodate the variable response of reactor-vessel materials in post-irradiation annealing at various temperatures and different time periods. Certain inherent limiting factors must be considered in developing an annealing procedure. These factors include system-design limitations; physical constraints resulting from attached piping, support structures, and the primary system shielding; the mechanical and thermal stresses in the components and the system as a whole; and, material condition changes that may limit the annealing temperature.

1.3?This guide provides direction for development of the vessel annealing procedure and a post-annealing vessel radiation surveillance program. The development of a surveillance program to monitor the effects of subsequent irradiation of the annealed-vessel beltline materials should be based on the requirements and guidance described in Practices E185 and E2215. The primary factors to be considered in developing an effective annealing program include the determination of the feasibility of annealing the specific reactor vessel; the availability of the required information on vessel mechanical and fracture properties prior to annealing; evaluation of the particular vessel materials, design, and operation to determine the annealing time and temperature; and, the procedure to be used for verification of the degree of recovery and the trend for reembrittlement. Guidelines are provided to determine the post-anneal reference nil-ductility transition temperature (1.4?The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.

1.5?This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6?This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.