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ASTM E1251-17a

Standard Test Method for Analysis of Aluminum and Aluminum Alloys by Spark Atomic Emission Spectrometry (Includes all amendments and changes 10/26/2017).

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NORMA vydána dne 1.10.2017

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Informace o normě:

Označení normy: ASTM E1251-17a
Datum vydání normy: 1.10.2017
Kód zboží: NS-798686
Počet stran: 10
Přibližná hmotnost: 30 g (0.07 liber)
Země: Americká technická norma
Kategorie: Technické normy ASTM

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Anotace textu normy ASTM E1251-17a :

Keywords:

aluminum, aluminum alloys, Spark Atomic Emission Spectrometry (Spark-AES),, ICS Number Code 77.120.10 (Aluminium and aluminium alloys)

Doplňující informace

Significance and Use

5.1 The metallurgical properties of aluminum and its alloys are highly dependent on chemical composition. Precise and accurate analyses are essential to obtaining desired properties, meeting customer specifications, and helping to reduce scrap due to off-grade material.

5.2 This test method is applicable to chill cast specimens as defined in Practices E716 and can also be applied to other types of samples provided that suitable reference materials are available. Also, other sample forms can be melted and cast into a disk, using an appropriate mold, as described in Practices E716. However, it should be noted that some elements (for example, magnesium) readily form oxides, while some others (for example, sodium, lithium, calcium, and strontium) are volatile, and may be lost to varying degrees during the melting process.

1. Scope

1.1 This test method describes the analysis of aluminum and its alloys by spark-atomic emission spectrometry (Spark-AES). The aluminum specimen to be analyzed may be in the form of a chill cast disk, casting, foil, sheet, plate, extrusion, or some other wrought form or shape. The elements covered in the scope of this method are listed in the table below.

Element

Tested Mass Fraction Range
(Wt %)

Antimony

0.001 to 0.003

Arsenic

0.001 to 0.006

Beryllium

0.0004 to 0.24

Bismuth

0.03 to 0.6

Boron

0.0006 to 0.009

Calcium

0.0002 to –

Chromium

0.001 to 0.23

Cobalt

0.4 to –

Copper

0.001 to 5.5

Gallium

0.02 to –

Iron

0.2 to 0.5

Lead

0.04 to 0.6

Lithium

0.0003 to 2.1

Magnesium

0.03 to 5.4

Manganese

0.001 to 1.2

Nickel

0.005 to 2.6

Phosphorus

0.003 to –

Silicon

0.07 to 16

Sodium

0.003 to 0.02

Strontium

0.03 to –

Tin

0.03 to –

Titanium

0.001 to 0.12

Vanadium

0.002 to 0.022

Zinc

0.002 to 5.7

Zirconium

0.001 to 0.12

Note 1: The mass fraction ranges given in the above scope were established through cooperative testing (ILS) of selected reference materials. The range shown for each element does not demonstrate the actual usable analytical range for that element. The usable analytical range may be extended higher or lower based on individual instrument capability, spectral characteristics of the specific element wavelength being used, and the availability of appropriate reference materials.

Note 2: Mercury (Hg) is intentionally not included in the scope. Analysis of Hg in aluminum by Spark-AES is not recommended. Accurate analysis of Hg using this technique is compromised by the presence of an intense iron interference. Inaccurate reporting of Hg due to these interference effects can jeopardize the current designation of aluminum production as a mercury-free process. To demonstrate compliance with legislated Hg content limits, use of an alternate method capable of analysis with a minimum reporting limit of 0.0001% or lower is recommended. Suitable techniques include but are not limited to GD-MS, XRF (X-ray fluorescence), cold vapor AA, and ICP-MS.

1.2 This test method is suitable primarily for the analysis of chill cast disks as defined in Practices E716. Other forms may be analyzed, provided that: (1) they are sufficiently massive to prevent undue heating, (2) they allow machining to provide a clean, flat surface, which creates a seal between the specimen and the spark stand, and (3) reference materials of a similar metallurgical condition and chemical composition are available.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

2. Referenced Documents

E305-21	Standard Practice for Establishing and Controlling Spark Atomic Emission Spectrochemical Analytical Curves
E406-19	Standard Practice for Using Controlled Atmospheres in Atomic Emission Spectrometry
E172-90(1999)	Practice for Describing and Specifying the Excitation Source in Emission Spectrochemical Analysis (Withdrawn 2001)
E158-86(1996)e1	Standard Practice for Fundamental Calculations to Convert Intensities into Concentrations in Optical Emission Spectrochemical Analysis (Withdrawn 2004)
E135-23a	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials (Includes all amendments and changes 7/17/2023).
E1329-10	Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019)
E876-89(1994)e1	Standard Practice for Use of Statistics in the Evaluation of Spectrometric Data (Withdrawn 2003)
E1507-98	Standard Guide for Describing and Specifying the Spectrometer of an Optical Emission Direct-Reading Instrument
E691-23	Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
E716-16(2021)e2	Standard Practices for Sampling and Sample Preparation of Aluminum and Aluminum Alloys for Determination of Chemical Composition by Spark Atomic Emission Spectrometry (Includes all amendments and changes 9/7/2022).
E826-14	Standard Practice for Testing Homogeneity of a Metal Lot or Batch in Solid Form by Spark Atomic Emission Spectrometry (Withdrawn 2023)

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