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Standard Test Method for Determination of 4-Carboxybenzaldehyde and p-Toluic Acid in Purified Terephthalic Acid by Capillary Electrophoresis with Reverse Voltage Mode
Automaticky přeložený název:
Standardní zkušební metoda pro stanovení 4-karboxybenzaldehydu a p-toluylovou kyselinou v přečištěné kyseliny tereftalové pomocí kapilární elektroforézy s zpětného chodu napětí
NORMA vydána dne 15.8.2013
Označení normy: ASTM D7881-13
Poznámka: NEPLATNÁ
Datum vydání normy: 15.8.2013
Kód zboží: NS-39231
Počet stran: 7
Přibližná hmotnost: 21 g (0.05 liber)
Země: Americká technická norma
Kategorie: Technické normy ASTM
Keywords:
capillary electrophoresis, purified terephthalic acid, 4-carboxybenzaldehyde, p-toluic acid, reverse voltage, ICS Number Code 71.080.40 (Organic acids)
Significance and Use | ||||||||||||||||
5.1 The presence of 4-CBA and 5.2 Determining the amount of 4-CBA and p-TOL remaining from the manufacture of PTA is often required. This test method is suitable for setting specifications and for use as an internal quality control where these products are produced or used. 5.3 This test method is intended as an alternative to the HPLC method for the determination of 4-CBA and p-TOL in PTA. The major benefits of CE are speed, simplicity, reduced reagent consumption, and operating costs. |
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1. Scope | ||||||||||||||||
1.1 This test method2 covers the determination of 4-carboxybenzaldehyde (4-CBA) and p-toluic acid (1.2 In determining the conformance of the test results using this method to applicable specification, results shall be rounded off in accordance with the rounding-off method of Practice E29. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. |
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2. Referenced Documents | ||||||||||||||||
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