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ASTM D7845-13

Standard Test Method for Determination of Chemical Species in Marine Fuel Oil by Multidimensional Gas Chromatography – Mass Spectrometry

Automaticky přeložený název:

Standardní zkušební metoda pro stanovení chemických látek v mořské topného oleje multidimenzionální plynové chromatografie & ndash; Hmotnostní spektrometrie

NORMA vydána dne 1.4.2013

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Informace o normě:

Označení normy: ASTM D7845-13
Poznámka: NEPLATNÁ
Datum vydání normy: 1.4.2013
Kód zboží: NS-39181
Počet stran: 11
Přibližná hmotnost: 33 g (0.07 liber)
Země: Americká technická norma
Kategorie: Technické normy ASTM

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Lodní motory a hnací systémy
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Anotace textu normy ASTM D7845-13 :

Keywords:

bunker fuel oil, gas chromatography, GC/MS, marine fuel oil, mass spectrometry, ICS Number Code 47.020.20 (Marine engines and propulsion systems), 75.160.20 (Liquid fuels)

Doplňující informace

Significance and Use

5.1 The test method allows the quantitation of chemical species at low levels in marine fuel oils and cutter stocks. A great many types and concentrations of chemical species are found in marine fuel oils. A root cause relationship between the presence of such species or their concentration in fuels and any failure modes allegedly induced by the use of these fuels has not been established. This method is necessary to establish test conditions required for future ISO 8217:2010 Petroleum products- Fuels (class F)-Specifications of marine fuel oils as defined in section 5.5 and Annex B item (d). Additional compounds may be determined by using the same conditions and by selecting required mass spectral selected ions, accordingly.

1. Scope

1.1 This test method covers the quantitative determination of a variety of chemical species in marine fuel oil (bunker fuel oil) by gas chromatography – mass spectrometry. By using the same conditions and by selecting required mass spectral selected ions, the test method may be used for the determination of other species than those for which precision statements and limits of detection have been established.

1.2 An example list of chemical species for which a limit of quantification has been determined by means of this test method is given in Table 1.

Limit of Quantitation
mg/kg

n-butyl alcohol

Cyclohexanol

n-butyl ether

n-butyl acylate

Styrene

alpha-pinene

Phenol

alpha-methyl styrene

beta-pinene

4-methyl styrene

trans-B-methyl styrene

3-methyl styrene

2-methyl styrene

Dicyclopentadiene

Limonene

Indene

1-phenyl ethanol

para, alpha-Dimethyl styrene

2,5 dimethyl styrene

2,4 dimethyl styrene

2-phenyl ethanol (phenylethanol)

2-Ethyl Phenol

2,4 Dimethyl Phenol

4-Ethyl Phenol (co elutes with 3-ethylphenol)

2-Phenoxy-1-propanol

2-Phenoxy ethanol

4-isopropylphenol

1-Phenoxy-2-Propanol

Styrene Glycol

1.3 Other refinery hydrocarbon fractions and their mixtures may be tested using the same test method conditions. However, the precision of this test method reflects the compounds in 1.4 Results are reported to the nearest 1.0 mg/kg.

1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents

D4307-17(2021)	Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
D6299-23a	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance (Includes all amendments and changes 12/12/2023).
ISO 8217:2010	Petroleum ProductsFuels (Class F)Specifications of Marine Fuels Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http://www.ansi.org.