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Standard Test Method for Determination of Bisphenol A in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry
Přeložit název
NORMA vydána dne 15.4.2023
Označení normy: ASTM D7574-23
Datum vydání normy: 15.4.2023
Kód zboží: NS-1145006
Počet stran: 10
Přibližná hmotnost: 30 g (0.07 liber)
Země: Americká technická norma
Kategorie: Technické normy ASTM
Keywords:
Bisphenol A, liquid chromatography, solid phase extraction, tandem mass spectrometry, water,, ICS Number Code 13.060.50 (Examination of water for chemical substances)
Significance and Use | ||||||||||||||||
5.1?The first reported synthesis of BPA was by the reaction of phenol with acetone by Zincke.5.2?The environmental source of BPA is predominantly from the decomposition of polycarbonate plastics and resins. BPA is not classified as bio-accumulative by the U.S. Environmental Protection Agency and will biodegrade. BPA has been reported to have adverse effects in aquatic organisms and may be released into environmental waters directly at trace levels through landfill leachate and POTW effluents. This method has been investigated for use with surface water and secondary and tertiary POTW effluent samples therefore, it is applicable to these matrices only. It has not been investigated for use with salt water or solid sample matrices. |
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1. Scope | ||||||||||||||||
1.1?This test method covers the determination of bisphenol A (BPA) extracted from water utilizing solid phase extraction (SPE), separated using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). BPA is qualitatively and quantitatively determined by this method. This test method adheres to multiple reaction monitoring (MRM) mass spectrometry. 1.2?The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3?The method detection limit (MDL) and reporting limit (RL) for BPA are listed in Table 1. 1.4?This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5?This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. |
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2. Referenced Documents | ||||||||||||||||
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