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ASTM D7485-16

Standard Test Method for Determination of Nonylphenol, p-tert-Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry

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NORMA vydána dne 1.2.2016

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Provedení	PDF - okamžité stažení - 2 047.00 Kč Tištěné - 2 047.00 Kč
Dostupnost	SKLADEM
Cena	2047.00 Kč bez DPH
2 047.00 Kč

Informace o normě:

Označení normy: ASTM D7485-16
Poznámka: NEPLATNÁ
Datum vydání normy: 1.2.2016
Kód zboží: NS-640227
Počet stran: 11
Přibližná hmotnost: 33 g (0.07 liber)
Země: Americká technická norma
Kategorie: Technické normy ASTM

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Kategorie - podobné normy:

Zkoušení chemických substancí vody

Anotace textu normy ASTM D7485-16 :

Keywords:

diethoxylate, liquid chromatography, monoethoxylate, nonylphenol, octylphenol, solid phase extraction, tandem mass spectrometry, water,, ICS Number Code 13.060.50 (Examination of water for chemical substances)

Doplňující informace

Significance and Use

5.1 NP and OP have been shown to have toxic effects in aquatic organisms. The source of NP and OP is prominently from the use of common commercial surfactants. The most widely used surfactant is nonylphenol ethoxylate (NPEO) which has an average ethoxylate chain length of nine. The ethoxylate chain is readily biodegraded to form NP1EO, NP2EO, nonylphenol carboxylate (NPEC) and, under anaerobic conditions, NP. NP will also biodegrade, but may be released into environmental waters directly at trace levels. This method has been investigated and is applicable for environmental waters, including seawater.

1. Scope

1.1 This test method covers the determination of nonylphenol (NP), nonylphenol ethoxylate (NP1EO), nonylphenol diethoxylate (NP2EO), and octylphenol (OP), extracted from water utilizing solid phase extraction (SPE), separated using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These compounds are qualitatively and quantitatively determined by this method. This method adheres to single reaction monitoring (SRM) mass spectrometry.

1.2 The method detection limit (MDL) and reporting limit (RL) for NP, NP1EO, NP2EO, and OP are listed in Table 1.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents

D1129-13(2020)e2	Standard Terminology Relating to Water (Includes all amendments and changes 2/14/2024).
D5847-22	Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
D5905-98(2018)	Standard Practice for the Preparation of Substitute Wastewater
The Code of Federal Regulations	40 CFR Part 136, Appendix B
D3856-11	Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
D3694-96(2017)	Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
D2777-21	Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
D1193-06(2018)	Standard Specification for Reagent Water

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