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ASTM D7343-12(2017)
Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
Přeložit název
NORMA vydána dne 1.6.2017
Informace o normě:
Označení normy: ASTM D7343-12(2017)
Poznámka: NEPLATNÁ
Datum vydání normy: 1.6.2017
Kód zboží: NS-688080
Počet stran: 7
Přibližná hmotnost: 21 g (0.05 liber)
Země: Americká technická norma
Kategorie: Technické normy ASTM
Kategorie - podobné normy:
Anotace textu normy ASTM D7343-12(2017) :
Keywords:
calibration, EDXRF, regression, validation, WDXRF,, ICS Number Code 71.040.50 (Physicochemical methods of analysis)
Doplňující informace
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3.1 Accurate elemental analyses of samples of petroleum and petroleum products are required for the determination of chemical properties, which are in turn used to establish compliance with commercial and regulatory specifications. |
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1.1 This practice covers information relating to sampling, calibration and validation of X-ray fluorescence instruments for elemental analysis, including all kinds of wavelength dispersive (WDXRF) and energy dispersive (EDXRF) techniques. This practice includes sampling issues such as the selection of storage vessels, transportation, and sub-sampling. Treatment, assembly, and handling of technique-specific sample holders and cups are also included. Technique-specific requirements during analytical measurement and validation of measurement for the determination of trace elements in samples of petroleum and petroleum products are described. For sample mixing, refer to Practice D5854. Petroleum products covered in this practice are considered to be a single phase and exhibit Newtonian characteristics at the point of sampling. 1.2 Applicable Test Methods—This practice is applicable to the XRF methods under the jurisdiction of ASTM Subcommittee D02.03 on Elemental Analysis, and those under the jurisdiction of the Energy Institute’s Test Method Standardization Committee (Table 1). Some of these methods are technically equivalent though they may differ in details (Table 2). TABLE 1 XRF Standard Test Methods for Analysis of Petroleum Products and Lubricants
TABLE 2 Technically Equivalent XRF Test Methods for Petroleum Products and LubricantsA
1.3 Applicable Fluids—This practice is
applicable to petroleum and petroleum products with vapor pressures
at sampling and storage temperatures less than or equal to 101 kPa
(14.7 psi). Use Practice D4057 or IP 475 to sample these
materials. Refer to Practice D5842 when sampling materials that also
require Reid vapor pressure (RVP) determination.
1.4 Non-applicable Fluids—Petroleum products whose vapor pressure at sampling and sample storage conditions are above 101 kPa (14.7 psi) and liquefied gases (that is, LNG, LPG, etc.) are not covered by this practice. 1.5 Sampling Methods—The physical sampling and methods of sampling from a primary source are not covered by this guide. It is assumed that samples covered by this practice are a representative sample of the primary source liquid. Refer to Practice D4057 or IP 475 for detailed sampling procedures. 1.6 The values stated in SI units are to be regarded as the standard. 1.6.1 Exception—The values given in parentheses are for information only. 1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. |
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