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Standard Test Method for Determination of the Oxidation of Used Lubricants by FT-IR Using Peak Area Increase Calculation (Includes all amendments And changes 12/16/2019).
Automaticky přeložený název:
Standardní zkušební metoda pro stanovení oxidaci použitá maziva, FT-IR Používání Peak Area Zvýšení výpočet
NORMA vydána dne 1.11.2012
Označení normy: ASTM D7214-07a(2012)
Poznámka: NEPLATNÁ
Datum vydání normy: 1.11.2012
Kód zboží: NS-37889
Počet stran: 8
Přibližná hmotnost: 24 g (0.05 liber)
Země: Americká technická norma
Kategorie: Technické normy ASTM
Keywords:
differential spectrum, FT-IR, in-service lubricant, lubricant, oxidation measurement, PAI, used oil, ICS Number Code 75.100 (Lubricants, industrial oils and related products)
Significance and Use | ||||||||||||||
5.1 The PAI is representative of the quantity of all the compounds containing a carbonyl function that have formed by the oxidation of the lubricant (aldehydes, ketones, carboxylic acids, esters, anhydrides, etc.). The PAI gives representative information on the chemical degradation of the lubricant which has been caused by oxidation. 5.2 This test method was developed for transmission oils and is used in the CEC L-48-A-00 test (Oxidation Stability of Lubricating Oils Used in Automotive Transmissions by Artificial Aging) as a parameter for the end of test evaluation. |
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1. Scope | ||||||||||||||
1.1 This test method covers the determination of the oxidation of used lubricants by FT-IR (Fourier Transform Infrared Spectroscopy). It measures the concentration change of constituents containing a carbonyl function that have formed during the oxidation of the lubricant. 1.2 This test method may be used to indicate relative changes that occur in an oil under oxidizing conditions. The test method is not intended to measure an absolute oxidation property that can be used to predict performance of an oil in service. 1.3 This test method was developed for transmission oils which have been degraded either in service, or in a laboratory test, for example a bulk oxidation test. It may be used for other in-service oils, but the stated precision may not apply. 1.4 The results of this test method may be affected by the presence of other components with an absorbance band in the zone of 1600–1800 cm-1. Low PAI values may be difficult to determine in those cases. Section 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. |
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2. Referenced Documents | ||||||||||||||
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