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Standard Test Method for p-Phenylenediamine Antidegradants Purity by Gas Chromatography
Automaticky přeložený název:
Standardní zkušební metoda pro p-fenylendiamin antidegradanty čistoty plynovou chromatografií
NORMA vydána dne 1.5.2012
Označení normy: ASTM D4937-96(2012)
Poznámka: NEPLATNÁ
Datum vydání normy: 1.5.2012
Kód zboží: NS-29204
Počet stran: 7
Přibližná hmotnost: 21 g (0.05 liber)
Země: Americká technická norma
Kategorie: Technické normy ASTM
Keywords:
antidegradant, antioxidant, antiozanant, gas chromatography, N-isopropyl-N`-phenyl-p-phenylenediamene (IPPD), N-(1,3 dimethylbutyl)-N`-phenyl-p-phenylenediamene (6PPD), N,N`bis-(14-dimethylpentyl)-p-phenylenediamene (77PD), N,N`-ditolyl-p-phenylenediamene (DTPD), phenylenediamene, p-phenylenediamene (PPD), ICS Number Code 71.040.30 (Chemical reagents)
Significance and Use | ||||||||||
This test method is designed to assess the relative purity of production PPDs. These additives are primarily used as antiozonants for tires and other rubber or polymeric products. Since the results of this test method are based on area normalization, it assumes that all components are eluted from the column and each component has the same detector response. Although this is not strictly true, the errors introduced are relatively small and much the same for all samples; thus, they can be ignored since the intent of the test method is to establish relative purity. Although trace amounts of “low boilers” are present in production samples, they are disguised by the solvent peak when using packed columns (Procedure A). |
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1. Scope | ||||||||||
1.1 This test method covers the determination of the purity of Class I, II, and III p-phenylenediamine (PPD) antidegradants as described in Classification D4676 by gas chromatography (GC) detection and area normalization for data reduction. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. |
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2. Referenced Documents | ||||||||||
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