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ASTM D7858-13

Standard Test Method for Determination of Bisphenol A in Soil, Sludge and Biosolids by Pressurized Fluid Extraction and Analyzed by Liquid Chromatography/Tandem Mass Spectrometry

Automaticky přeložený název:

Standardní zkušební metoda pro stanovení bisfenolu A v půdě, kalů a biohmoty stlačeným fluidní extrakce a analyzovány kapalinová chromatografie / Tandem hmotnostní spektrometrie

NORMA vydána dne 1.4.2013

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Informace o normě:

Označení normy: ASTM D7858-13
Poznámka: NEPLATNÁ
Datum vydání normy: 1.4.2013
Kód zboží: NS-39194
Počet stran: 11
Přibližná hmotnost: 33 g (0.07 liber)
Země: Americká technická norma
Kategorie: Technické normy ASTM

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Kategorie - podobné normy:

Chemické charakteristiky půd

Anotace textu normy ASTM D7858-13 :

Keywords:
bisphenol A, liquid chromatography, mass spectrometry, pressurized fluid extraction, soil, ICS Number Code 13.080.10 (Chemical characteristics of soil)

Doplňující informace

Significance and Use

5.1 This is a performance based method, and modifications are allowed to improve performance.

5.1.1 Due to the rapid development of newer instrumentation and column chemistries, changes to the analysis described in this test method are allowed as long as better or equivalent performance data result. Any modifications shall be documented and performance data generated. The user of the data generated by this test method shall be made aware of these changes and given the performance data demonstrating better or equivalent performance.

5.2 The first reported synthesis of BPA was by the reaction of phenol with acetone by Zincke.5.3 The environmental source of BPA is predominantly from the decomposition of polycarbonate plastics and resins. BPA is not classified as bio-accumulative by the U.S. Environmental Protection Agency and will biodegrade. BPA has been reported to have adverse effects in aquatic organisms and may be released into environmental waters directly at trace levels through landfill leachate and sewage treatment plant effluents. This method has been investigated for use with soil, sludge, and biosolids.

5.4 The land application of biosolids has raised concerns over the fate of BPA in the environment and a standard method is needed to monitor concentrations. This method has been investigated for use with various soils.

1. Scope

1.1 This procedure covers the determination of Bisphenol A (BPA) in soil, sludge, and biosolids. This test method is based upon solvent extraction of a soil matrix by pressurized fluid extraction (PFE). The extract is filtered and analyzed by liquid chromatography/tandem mass spectrometry (LC/MS/MS). BPA is qualitatively and quantitatively determined by this test method.

1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 The Method Detection Limit

Analyte

ESI Mode

MDL (PPB)

Reporting Range (PPB)

Bisphenol A

Negative

2.8

10-250

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents

D653-22	Standard Terminology Relating to Soil, Rock, and Contained Fluids
D1193-06(2018)	Standard Specification for Reagent Water
D3694-96(2017)	Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
D3740-23	Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
D3856-11	Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
D5681-23	Standard Terminology for Waste and Waste Management
E2554-18e1	Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques (Includes all amendments and changes 10/7/2019).